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    ASTM A1082/A1082M Bolting Specification

    High Strength Precipitation Hardening and Duplex Stainless Steel Bolting for Special Purpose Applications

    ASTM A1082/A1082M Hex Bolts, Heavy Hex Bolts, Studs, Socket Head Cap Screws, Threaded Rods

    ASTM A1082/A1082M (2016 edition) covers high strength stainless steel bolting materials and bolting components, including bars, bolts and nuts, for special purpose applications such as pressure vessels. It lists 14 duplex (ferritic-austenitic) grades and 5 precipitation-hardening grades; selection depends on design, service conditions, mechanical properties and characteristics related to the application. Specification A962/A962M is indispensable and applies in full, but A1082 prevails where the two conflict (clauses 1.2 and 4.1). Inch-pound units apply unless the order specifies the A1082M (SI) designation (clause 1.4). Bars shall be produced in accordance with Specifications A276/A276M, A479/A479M or A564/A564M as applicable. Finish (hot or cold, ground, rough turned, drawn, etc.) shall be at the option of the manufacturer unless otherwise specified in the purchase order or contract.

    Ordering and heat treatment. PH bolting ordered to a Type or UNS designation only is supplied solution treated per Table 2; ordered to a Type and Condition (for example Type 630 H1150) it must meet the age-hardened requirements of Table 3 (clause 7.1.1). Duplex bolting is furnished solution annealed per Table 4 (clause 7.2.1). Hardness is tested after all production heat treatment: one test on each mill-treated length for bars 2 in. [50 mm] and over, and on at least 10 % of the lengths under 2 in. (clause 8.4). The certification report gives the chemical analysis, mechanical test results and the heat treatment method (clause 10.1).

    ASTM A1082/A1082M Chemical RequirementsA

    Grades UNSDesignationB TypeB C Mn P S Si Cr Ni Mo N Other Elements
    ASTM A1082/A1082M Austenitic Stainless Steel Grades S31100 . . . 0.06 1.00 0.045 0.030 1.00 25.0-27.0 6.0-7.0 . . . . . . Ti 0.25
    ASTM A1082/A1082M Super Austenitic Stainless Steel GradesS31260 . . . 0.030 1.00 0.030 0.030 0.75 24.0-26.0 5.5-7.5 2.5-3.5 0.10-0.30 Cu 0.20-0.80,W 0.10-0.50
    ASTM A1082/A1082M Duplex (Ferritic-Austenitic) GradesS31803 . . . 0.030 2.00 0.030 0.020 1.00 21.0-23.0 4.5-6.5 2.5-3.5 0.08-0.20 . . .
    S32101 . . . 0.040 4.0-6.0 0.040 0.030 1.00 21.0-22.0 1.35-1.70 0.10-0.80 0.20-0.25 Cu 0.10-0.80
    S32202 . . . 0.030 2.00 0.040 0.010 1.00 21.5-24.0 1.0-2.80 0.45 0.18-0.26 . . .
    S32205 2205 0.030 2.00 0.030 0.020 1.00 22.0-23.0 4.5-6.5 3.0-3.5 0.14-0.20 . . .
    S32304 2304 0.030 2.50 0.040 0.030 1.00 21.5-24.5 3.0-5.5 0.05-0.60 0.05-0.20 Cu 0.05-0.60
    S32506 . . . 0.030 1.00 0.040 0.015 0.90 24.0-26.0 5.5-7.2 3.0-3.5 0.08-2.0 W 0.05-0.30
    S32550 255 0.040 1.50 0.040 0.030 1.00 24.0-27.0 4.5-6.5 2.9-3.9 0.10-0.25 Cu 1.50-2.50
    S32750 2507 0.030 1.20 0.035 0.020 0.80 24.0-26.0 6.0-8.0 3.0-5.0 0.24-0.32 Cu 0.50
    S32760 . . . 0.030 1.00 0.030 0.010 1.00 24.0-26.0 6.0-8.0 3.0-4.0 0.20-0.30 Cu 0.50-1.00,W 0.50-1.00,%Cr+3.3x%Mo +16x%N≥40
    S32906 . . . 0.030 0.80-1.50 0.030 0.030 0.50 28.0-30.0 5.8-7.5 1.50-2.60 0.30-0.40 Cu 0.80
    S32950 . . . 0.030 2.00 0.035 0.010 0.60 26.0-29.0 3.5-5.2 1.00-2.50 0.15-0.35 . . .
    ASTM A1082/A1082M Super Austenitic Stainless Steel GradesS39277 . . . 0.025 0.80 0.025 0.002 0.80 24.0-26.0 6.5-8.0 3.0-4.0 0.23-.033 Cu 1.20-2.00,W 0.80-1.20
    ASTM A1082/A1082M Precipitation Hardening Grades S15700 632 0.09 1.00 0.040 0.030 1.00 14.0-16.0 6.5-7.7 2.00-3.00 . . . Al 0.75-1.50
    S17400 630 0.07 1.00 0.040 0.030 1.00 15.0-17.0 3.0-5.0 . . . . . . Cu 3.0-5.0,Cb +Ta 0.15-0.45
    S17600 635 0.08 1.00 0.040 0.030 1.00 16.0-17.5 6.0-7.5 . . . . . . Al 0.40,Ti 0.40-1.20
    S17700 631 0.09 1.00 0.040 0.030 1.00 16.0-18.0 6.5-7.7 . . . . . . Al 0.75-1.50
    S35500 634 0.10-0.15 0.50-1.25 0.040 0.030 0.50 15.0-16.0 4.0-5.0 2.5-3.2 0.07-0.13 Cb 0.10-0.50
    • (A)Maximum or range unless otherwise indicated.
    • (B)See GuideA959/A959M.

    ASTM A1082/A1082M Solution Treatment and Mechanical Property Requirements for PH Grades

    UNSDesignation Type Solution TreatmentB, C°F [°C] Mechanical Property Requirements in the Solution Treated Condition
    Tensile Strengthksi [MPa] Yield Strengthksi [MPa] Elongation in 2"[50 mm]or 4D,min. % Reduction of Area,min. % HardnessD
    Rockwell,maximum Brinell,maximum
    S15700 632 . . . . . . . . . . . . . . . 100 HRB 269
    S17400 630 Cool to below 90 [32] . . . . . . . . . . . . 38 HRC 363
    S17600 635 Air Cool 120 [825] 75 [515] 10 45 32 HRC 302
    S17700 631 . . . . . . . . . . . . . . . 98 HRB 229
    S35500 634 Hold at≤-100 [-73] for atleast 3 hours . . . . . . . . . . . . . . . 363
    • (A)Values shown are minimums or ranges unless maximum is indicated.
    • (B)1900 [1040] ± 25°F [15°C].
    • (C)Quenched in water unless the table specifies another media.
    • (D)Either Rockwell or Brinell testing is permitted unless thickness is below1/2" in which case Rockwell is preferred.

    ASTM A1082/A1082M Age Hardening Treatment and Mechanical Property Requirements for PH GradesA

    Type Condition Suggested Hardeningand/or AgingTemperatures, Timeat Temperature,and Quench Media°F [°C]B,C,D,E Maximum Thickness inch [mm] inclusive Mechanical Properties
    TensileStrength ksi [MPA] YieldStrengthksi [MPA] Elongation in 2"[50 mm] or 4D% Reduction of Area,% HardnessF Impact Ft-lbf [J]
    Rockwell, HRC Brinell
    630 H900 900 [480], 1 hour 8 190 [1310] 170 [1170] 10 35 40 388 . . .
    630 H925 925 [495], 4 hours 8 170 [1170] 155 [1070] 10 38 38 375 5 [6.8]
    630 h4025 1025 [550], 4 hours 8 155 [1070] 145 [1000] 12 45 35 331 15 [20]
    630 h4075 1075 [580], 4 hours 8 145 [1000] 125 [860] 13 45 32 311 20 [27]
    630 h4100 1100 [595], 4 hours 8 140 [965] 115 [795] 14 45 31 302 25 [34]
    630 h4150 1150 [620], 4 hours 8 135 [930] 105 [725] 16 50 28 277 30 [41]
    630 h4150D 1150 [620] for 4 hrs., air cool plus 1150 [620] for 4 hrs., air cool 8 125 [860] 105 [725] 16 50 24-33 255-311 30 [41]
    630 h4150M 1400 [760] for 2 hrs., air cool plus 1150 [620] for 4 hrs., air cool 8 115 [795] 75 [520] 18 55 24 255 55 [75]
    631 RH950 1750 [955] for 10 min. to 1 h, rapidly cool to room temperature. Cool within 24 hrs. to -100 ± 10 [-75 ± 5], hold 8 hrs. min. Warm in air to room temperature. Heat to 950 [510] hold 1 h, air cool. 4 185 [1280] 150 [1030] 6 10 41 388 . . .
    631 Th4050 1400 [760] for 90 min. Cool to 55 ± 5 [15 ± 3] within 1 h, hold1/2h min., heat to 1050 [565], hold for 90 min., air cool 6 170 [1170] 140 [965] 6 25 38 352 . . .
    632 RH950 Same as Type 631 4 200 [1380] 175 [1210] 7 25 44 415 . . .
    632 Th4050 Same as Type 631 6 180 [1240] 160 [1100] 8 25 38 375 . . .
    634 h4000 1750 [955] for 10 min. to 1 h, water quench. Cool to -100 [75] min., hold 3 hrs. min. Temper at 1000 [540] hold for 3 h min, air cool. . . . 170 [1170] 155 [1070] 12 25 37 341 . . .
    635 H950 950 [510],1/2h . . . 190 [1310] 170 [1170] 8 25 39 363 . . .
    635 h4000 1000 [540],1/2h . . . 180 [1240] 160 [1100] 8 30 37 352 . . .
    635 h4050 1050 [565],1/2h . . . 170 [1170] 150 [1035] 10 40 35 331 . . .
    • (A)Values shown are minimums or ranges unless maximum is indicated.
    • (B)± 25°F [15°C]
    • (C)Temperatures are suggested and may be varied to obtain the required tensile properties.
    • (D)Time refers to the minimum time the material is at temperature and may be extended to obtain required ductility properties.
    • (E)Quenching shall be accomplished using air or gas cooling unless the table specifies another media.
    • (F)Either Rockwell or Brinell testing is permitted unless thickness is below1/2" in which case Rockwell is preferred.

    ASTM A1082/A1082M Heat Treatment and Mechanical Property Requirements for Duplex GradesA

    UNSDesignation Solution Temperature,°F [°C]B,C Size Range Mechanical Properties
    TensileStrength,ksi [MPA] YieldStrength,ksi [MPA] Elongation in 2"[50 mm] or 4D% HardnessD
    Rockwell, HRC maximum Brinell,maximum
    S31100 1900 [1040] . . . 90 [620] 65 [450] 20 30 290
    ASTM A1082/A1082M Super Austenitic Stainless Steel GradesS31260 1870 to 2010 [1020 to 1100] . . . 100 [690] 70 [485] 20 31 297
    ASTM A1082/A1082M Duplex (Ferritic-Austenitic) GradesS31803 1900 [1040] . . . 90 [620] 65 [450] 25 30 290
    S32101 1870 [1020] . . . 94 [650] 65 [450] 30 30 290
    S32202 1800 to 1975 [980 to 1080] . . . 94 [650] 65 [450] 30 30 290
    S32205 1900 [1040] . . . 95 [655] 65 [450] 25 30 290
    S32304 1800 [980] . . . 90 [620] 65 [450] 18 32 302
    S32506 1870 - 2050 [1020 - 1120] . . . 90[620] 65 [450] 18 32 302
    S32550 1900 [1040] . . . 110[760] 80 [550] 15 31 297
    S32750 1880 - 2060 [1025 - 1125] 2 in. and under 116[800] 80 [550] 15 33 310
    >2 in. 110 [760] 75 [515] 15 33 310
    S32760 2010 [1100] . . . 109 [750] 80 [550] 25 30 290
    S32900 1750 [955] . . . 90 [620] 70 [485] 15 30 290
    S32906 1830 to 2100 [1000 to 1150] . . . 109 [750] 80 [550] 25 33 310
    • (A)Values shown are minimums or ranges unless maximum is indicated.
    • (B)± 25°F [15°C].
    • (C)Quenched in water.
    • (D)Either Rockwell or Brinell testing is permitted unless thickness is below1/2" in which case Rockwell is preferred.

    ASTM A1082/A1082M Markings

    Grades UNS Designation Type Condition Grade Symbol
    ASTM A1082/A1082M Austenitic Stainless Steel Grades S31100 . . . . . . TB 31100
    ASTM A1082/A1082M Super Austenitic Stainless Steel GradesS31260 . . . . . . TB 31260
    ASTM A1082/A1082M Duplex (Ferritic-Austenitic) GradesS31803 . . . . . . TB 31803
    S32101 . . . . . . TB 32101
    S32202 . . . . . . TB 32202
    S32205 2205 . . . TB 32205
    S32304 2304 . . . TB 32304
    S32506 . . . . . . TB 32506
    S32550 255 . . . TB 32550
    S32750 2507 . . . TB 32750
    S32760 . . . . . . TB 32760
    S32900 . . . . . . . . .
    S32906 . . . . . . TB 32906
    ASTM A1082/A1082M Precipitation Hardening Grades S15700 632 . . . TB 157
    S15700 632 RH95 TB 157A
    S15700 632 Th4050 TB 157B
    S17400 630 . . . TB 174
    S17400 630 H900 TB 174A
    S17400 630 H925 TB 174B
    S17400 630 h4025 TB 174C
    S17400 630 h4075 TB 174D
    S17400 630 h4100 174E
    S17400 630 h4150 TB 174G
    S17400 630 h4150D TB 174H
    S17400 630 h4150M 174J
    S17600 635 . . . TB 176
    S17600 635 H950 TB 176A
    S17600 635 h4000 TB 176B
    S17600 635 h4050 TB 176C
    S17700 631 . . . TB 177
    S17700 631 RH95 TB 177A
    S17700 631 Th4050 TB 177B
    S35500 634 . . . TB 355
    S35500 634 h4000 TB 355A

    ASTM A1082/A1082M Supplementary Requirements

    Supplementary requirements apply only when the purchaser specifies them individually in the purchase order or contract (clause 1.3).

    S1 Charpy Impact Tests

    When S1 is specified, Charpy impact testing is required and the samples shall meet the impact values of Table 3, which lists them for Type 630 from H925 (5 ft-lbf [6.8 J]) to H1150M (55 ft-lbf [75 J]).

    S2 Product Marking

    With S2, the grade symbol from Table 5 (for example 174A for S17400 in H900) is applied to one end of studs and to the heads of bolts of all sizes. If the area is too small, the grade symbol may go on one end and the manufacturer's identification on the other. Bolts under 1/4 in. [6 mm], studs under 3/8 in. [10 mm] and 1/4 in. [6 mm] studs that need more than three symbols are marked by agreement.

    S3 Stress Relieving

    If material is straightened after heat treatment, a stress-relieving operation shall follow, 50 to 100 °F [28 to 55 °C] below the tempering temperature. Mechanical property tests are performed after stress relieving.

    S4 Non-Destructive Inspection

    Each bar or forged blank of starting material is examined after final heat treatment by eddy current, magnetic particle (wet or dry), liquid penetrant, ultrasonic or visual testing, at the producer's option. With MPI or LPI, linear indications longer than 1/16 in. [1.5 mm] and longer than three times their width are unacceptable. UT and ET reject levels are set by a calibration notch no deeper than 0.012 in. [0.30 mm]. Product for visual testing is pickled first, and visual indications longer than 1/8 in. [3.2 mm] are prohibited. UT personnel are qualified to ASNT SNT-TC-1A (2006 or later) or an agreed national standard.

    S5 Proof Load Testing

    S5 requires proof load testing of nuts. The number of tests and the proof loads are agreed between purchaser and manufacturer.

    S6 Cross-Sectional Hardness Testing on Nuts

    S6 requires cross-sectional hardness testing of nuts in accordance with Annex A3 of ASTM A370, with the number of tests agreed between purchaser and manufacturer.

    Frequently Asked Questions

    What is ASTM A1082/A1082M?

    ASTM A1082/A1082M is the Standard Specification for High Strength Precipitation Hardening and Duplex Stainless Steel Bolting for Special Purpose Applications. The current extracted edition is 2016. It covers bolting materials and components such as bars, bolts and nuts for special purpose applications such as pressure vessels, with ASTM A962/A962M as its indispensable general requirements.

    Which grades does ASTM A1082 cover?

    ASTM A1082/A1082M (2016) Table 1 lists 14 duplex (ferritic-austenitic) grades, S31100, S31260, S31803, S32101, S32202, S32205 (2205), S32304 (2304), S32506, S32550 (255), S32750 (2507), S32760, S32906, S32950 and S39277, and 5 precipitation-hardening grades, S15700 (Type 632), S17400 (Type 630), S17600 (Type 635), S17700 (Type 631) and S35500 (Type 634). Grade selection depends on design, service conditions and the mechanical properties required.

    What strength does 17-4 PH (Type 630) reach under ASTM A1082?

    Table 3 gives Type 630 minimums from H900 (tensile 190 ksi [1310 MPa], yield 170 ksi [1170 MPa], 10 % elongation) through H1025 (155 ksi [1070 MPa], 145 ksi [1000 MPa]) and H1150 (135 ksi [930 MPa], 105 ksi [725 MPa], impact 30 ft-lbf [41 J]) to H1150M (115 ksi [795 MPa], 75 ksi [520 MPa], impact 55 ft-lbf [75 J]), for sections up to 8 in.

    How is ASTM A1082 17-4 PH bolting heat treated?

    Solution treatment is 1900 °F [1040 °C] ±25 °F [15 °C] with cooling to below 90 °F [32 °C] (Table 2). Table 3 then gives the suggested ageing: H900 at 900 °F [480 °C] for 1 hour; H925, H1025, H1075, H1100 and H1150 for 4 hours at 925 to 1150 °F [495 to 620 °C]; H1150D, 1150 °F [620 °C] for 4 hours twice; H1150M, 1400 °F [760 °C] for 2 hours then 1150 °F [620 °C] for 4 hours, each air cooled.

    What are the super duplex 2507 (S32750) requirements?

    Table 4: solution annealed at 1880 to 2060 °F [1025 to 1125 °C], water quenched. Up to and including 2 in.: tensile 116 ksi [800 MPa] and yield 80 ksi [550 MPa] min. Over 2 in.: 110 ksi [760 MPa] and 75 ksi [515 MPa] min. Elongation 15 % min and hardness 33 HRC or 310 HB max for both. The marking grade symbol is 32750 (Table 5).

    Can ASTM A1082 bolting be used in sour service (NACE MR0175 / ISO 15156)?

    ISO 15156-3 Table A.24 accepts wrought duplex stainless steel for any equipment when it is solution-annealed and liquid-quenched or rapidly cooled, has 35 % to 65 % ferrite and has had no ageing heat treatment. With 30 ≤ PREN ≤ 40 and Mo ≥ 1.5 % the limit is 232 °C (450 °F) and 10 kPa (1.5 psi) H2S partial pressure; with 40 < PREN ≤ 45 it is 232 °C (450 °F) and 20 kPa (3 psi). Table A.27 accepts wrought 17-4 PH (S17400) at 33 HRC max after a double age at 620 °C (1150 °F) or a modified double age, for named wellhead, valve and subsurface components, up to 3.4 kPa (0.5 psi) H2S and pH 4.5 or above.

    Which supplementary requirements can be ordered?

    Six, each only when the purchaser specifies it (clause 1.3): S1 Charpy impact tests, S2 product marking, S3 stress relieving, S4 non-destructive inspection, S5 proof load testing of nuts and S6 cross-sectional hardness testing of nuts.